<\/p>\n

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1950\u5e74\u4ee3\u4e2d\u671f\uff0c\u53d1\u5c55\u4e861H-NMR\uff0c19F-NMR\u548c31P-NMR\u3002\u7b2c\u4e09\u9636\u6bb5\uff1a60-70\u5e74\uff0cNMR\u6280\u672f\u7684\u8de8\u8d8a\u671f\u3002\u8109\u51b2\u5085\u7acb\u53f6\u53d8\u6362\u6280\u672f\u63d0\u9ad8\u4e86\u7075\u654f\u5ea6\u548c\u5206\u8fa8\u7387\uff0c\u53ef\u5e38\u89c4\u6d4b\u91cf13C\u6838\uff1b\u53cc\u9891\u548c\u591a\u9891\u5171\u632f\u6280\u672f\uff1b\u7b2c\u56db\u9636\u6bb5\uff1a1970\u5e74\u4ee3\u540e\u671f\u7406\u8bba\u548c\u6280\u672f\u53d1\u5c55\u6210\u719f\u30021200\u3001300\u3001500\u3001500 MHz\u548c600 MHz\u8d85\u5bfcNMR\u5149\u8c31\u4eea\uff1b 2\uff0c\u5404\u79cd\u8109\u51b2\u7cfb\u5217\u7684\u5e94\u7528\uff0c\u5728\u5e94\u7528\u4e2d\u53d8\u5f97\u91cd\u8981\u53d1\u5c55\uff1b 3\uff0c\u4e8c\u7ef4\u6838\u78c1\u5171\u632f\u7684\u51fa\u73b0\uff1b 4\uff0c\u591a\u6838\u7814\u7a76\uff0c\u53ef\u5e94\u7528\u4e8e\u6240\u6709\u78c1\u82af\uff1b 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\/2\u03c0\uff09\u03b3\u00b7H\uff1b\u5728\u4e00\u5b9aH0\u4e0b\uff0c\u4e00\u4e2a\u539f\u5b50\u6838\u53ea\u6709\u4e00\u4e2a\u0394E\u0394E= E\u4e4b\u5916=h\u03bd\u552f\u4e00\u7684\u5438\u6536\u9891\u7387\u03bd\u4f8b\u5982H0 = 2.3500 T\uff0c1H\u7684\u5438\u6536\u9891\u7387\u4e3a100 MHz\uff0c13C\u7684\u5438\u6536\u9891\u7387\u4e3a25.2MHz\u2461\u2461\u771f\u6b63\u7684\u6838\uff1a\u5c4f\u853d\u73b0\u8c61\u7535\u5b50\u5916\u7684\u6838\uff08\u672a\u9694\u79bb\uff0c\u672a\u66b4\u9732\uff09\u5728\u5316\u5408\u7269\u4e2d\uff1a\u539f\u5b50\u95f4\u7684\u952e\u5408\uff08\u4f5c\u7528\uff09\u4e0d\u540c\uff0c\u4f8b\u5982\u5316\u5b66\u952e\uff0c\u6c22\u952e\u60f3\u8c61\u4e00\u4e0b\uff0c\u9759\u7535\u76f8\u4e92\u4f5c\u7528\uff0c\u5206\u5b50\u95f4\u4f5c\u7528\u529b\u60f3\u8c61\uff1a\u5728H0 = 2.3500 T\u65f6\uff0c\u7531\u4e8e\u5c4f\u853d\u5c42\u7684\u5916\u90e8\u7535\u5b50\uff0c\u5728\u6838\u4f4d\u7f6e\uff0c\u5b9e\u9645\u78c1\u573a\u7565\u5c0f\u4e8e2.3500 TR\u3002\u58f0\u5b50\u9891\u7387\u7565\u9ad8\u4e8e100 MHz\u591a\u5c11\uff1f 1H\u662f0\u523010\uff0c13C\u662f0\u5230250\u6c22\u6838\u5728\u5916\u9762\u6709\u7535\u5b50\uff0c\u5b83\u4eec\u6392\u65a5\u78c1\u573a\u7684\u78c1\u529b\u7ebf\u3002\u5bf9\u4e8e\u539f\u5b50\u6838\uff0c\u5468\u56f4\u7684\u7535\u5b50\u88ab\u5c4f\u853d\uff08Shielding\uff09\u6548\u5e94\u3002\u56f4\u7ed5\u82af\u7684\u7535\u5b50\u4e91\u7684\u5bc6\u5ea6\u8d8a\u5927\uff0c\u5c4f\u853d\u6548\u679c\u8d8a\u597d\uff0c\u76f8\u5e94\u7684\u78c1\u573a\u5f3a\u5ea6\u4e5f\u4f1a\u589e\u52a0\uff0c\u4ece\u800c\u4f7f\u5176\u5171\u632f\u3002\u539f\u5b50\u6838\u5468\u56f4\u7684\u7535\u5b50\u4e91\u5bc6\u5ea6\u53d7\u8fde\u63a5\u57fa\u56e2\u7684\u5f71\u54cd\uff0c\u56e0\u6b64\u4e0d\u540c\u5316\u5b66\u73af\u5883\u7684\u539f\u5b50\u6838\u53d7\u5230\u4e0d\u540c\u7684\u5c4f\u853d\u4f5c\u7528\uff0c\u5176\u6838\u78c1\u5171\u632f\u4fe1\u53f7\u4e5f\u51fa\u73b0\u5728\u4e0d\u540c\u7684\u4f4d\u7f6e\u3002\u2462\u5982\u679c\u4eea\u5668\u4ee560MHz\u6216\u5728100MHz\u4eea\u5668\u4e2d\uff0c\u6709\u673a\u5316\u5408\u7269\u8d28\u5b50\u7684\u7535\u78c1\u6ce2\u9891\u7387\u7ea6\u4e3a1000Hz\u62161700Hz\u3002\u5728\u786e\u5b9a\u7ed3\u6784\u65f6\uff0c\u9700\u8981\u786e\u5b9a\u6b63\u786e\u7684\u8c10\u632f\u9891\u7387\uff0c\u901a\u5e38\u9700\u8981\u51e0\u4e2aHz\u7684\u7cbe\u5ea6\uff0c\u901a\u5e38\u4ee5\u9002\u5f53\u7684\u5316\u5408\u7269\u4e3a\u6807\u51c6\u6765\u786e\u5b9a\u76f8\u5bf9\u9891\u7387\u3002\u6807\u51c6\u5316\u5408\u7269\u7684\u5171\u632f\u9891\u7387\u4e0e\u8d28\u5b50\u7684\u5171\u632f\u9891\u7387\u4e4b\u5dee\u79f0\u4e3a\u5316\u5b66\u4f4d\u79fb5\u3002 1 H NMR\u5149\u8c31\u4fe1\u606f\u4fe1\u53f7\u6570\u91cf\uff1a\u5206\u5b50\u4e2d\u5b58\u5728\u591a\u5c11\u79cd\u4e0d\u540c\u7c7b\u578b\u7684\u8d28\u5b50\u4fe1\u53f7\u7684\u4f4d\u7f6e\uff1a\u6bcf\u4e2a\u8d28\u5b50\u7684\u7535\u5b50\u73af\u5883\uff0c\u5316\u5b66\u4f4d\u79fb\u4fe1\u53f7\u5f3a\u5ea6\uff1a\u6bcf\u4e2a\u8d28\u5b50\u7684\u6570\u91cf\u6216\u6570\u91cf\u5206\u88c2\u60c5\u51b5\uff1a\u591a\u5c11\u5b58\u5728\u4e0d\u540c\u7684\u8d28\u5b50\u5e38\u89c1\u7c7b\u578b\u7684\u6709\u673a\u5316\u5408\u7269\u7684\u5316\u5b66\u4f4d\u79fb\u2460\u8bf1\u5bfc\u4f5c\u7528\u2461\u5171\u8f6d\u6548\u5e94\u7531\u4e8e\u03c0\u7535\u5b50\u7684\u4f4d\u79fb\uff0c\u8d28\u5b50\u5c4f\u853d\u4f1a\u51cf\u5f31\u6216\u589e\u5f3a\u5171\u8f6d\u4f5c\u7528\u2462\u5404\u5411\u5f02\u6027\u6548\u5e94\u5f88\u96be\u89e3\u91caH\u76f8\u5bf9\u4e8e\u03c0\u7535\u5b50\u7684\u5316\u5b66\u4f4d\u79fb\uff0c\u5e76\u4e14\u5f88\u96be\u89e3\u91ca\u7535\u8d1f\u6027\u2463H\u952e\u6548\u5e94ROH\uff0cRNH2\u57280.5-5\uff0cArOH\u57284-7\uff0c\u53d8\u5316\u8303\u56f4\uff0c\u8bb8\u591a\u56e0\u7d20\u7684\u5f71\u54cd\uff1b\u6c22\u952e\u968f\u6e29\u5ea6\uff0c\u6eb6\u5242\uff0c\u6d53\u5ea6\u7684\u53d8\u5316\u660e\u663e\uff0c\u53ef\u4ee5\u4e86\u89e3\u4e0e\u6c22\u952e\u6709\u5173\u7684\u7ed3\u6784\u548c\u53d8\u5316\u3002\u2464\u6eb6\u5242\u4f5c\u7528\u82ef\u4e0eDMF\u5f62\u6210\u914d\u5408\u7269\u3002\u82ef\u73af\u7684\u7535\u5b50\u4e91\u5438\u5f15DMF\u7684\u6b63\u6781\uff0c\u800c\u62d2\u7edd\u8d1f\u6781\u3002 \u03b1\u7532\u57fa\u5728\u5c4f\u853d\u533a\uff0c\u5171\u632f\u79fb\u5411\u9ad8\u573a\uff1b \u03b2\u7532\u57fa\u4f4d\u4e8e\u63a9\u853d\u533a\u57df\uff0c\u5171\u632f\u5438\u6536\u5411\u4f4e\u7535\u573a\u79fb\u52a8\uff0c\u5176\u7ed3\u679c\u662f\u4e24\u4e2a\u5438\u6536\u5cf0\u7684\u4f4d\u7f6e\u4e92\u6362\u3002
\n\u8d44\u6599\u6765\u6e90\uff1aMeeyou Carbide<\/p>\n

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First, the development of a brief historyThe first stage: 1945 to 1951, the invention of nuclear magnetic resonance and lay the theoretical and experimental basis of the period: Bloch (Stanford University, observed in the water proton signal) and Purcell (Harvard University, observed in the paraffin proton signal) obtained Nobel bonus.The second stage: 1951 to 1960…<\/p>","protected":false},"author":1,"featured_media":1601,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"_jetpack_memberships_contains_paid_content":false,"footnotes":""},"categories":[79,1],"tags":[],"class_list":["post-18529","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-materials-weekly","category-uncategorized"],"jetpack_featured_media_url":"https:\/\/www.meetyoucarbide.com\/wp-content\/uploads\/2019\/05\/f875f9_bb1c35716b08473c98191e3de498a58fmv2.png","jetpack_sharing_enabled":true,"_links":{"self":[{"href":"https:\/\/www.meetyoucarbide.com\/zh\/wp-json\/wp\/v2\/posts\/18529","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/www.meetyoucarbide.com\/zh\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/www.meetyoucarbide.com\/zh\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/www.meetyoucarbide.com\/zh\/wp-json\/wp\/v2\/users\/1"}],"replies":[{"embeddable":true,"href":"https:\/\/www.meetyoucarbide.com\/zh\/wp-json\/wp\/v2\/comments?post=18529"}],"version-history":[{"count":0,"href":"https:\/\/www.meetyoucarbide.com\/zh\/wp-json\/wp\/v2\/posts\/18529\/revisions"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/www.meetyoucarbide.com\/zh\/wp-json\/wp\/v2\/media\/1601"}],"wp:attachment":[{"href":"https:\/\/www.meetyoucarbide.com\/zh\/wp-json\/wp\/v2\/media?parent=18529"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/www.meetyoucarbide.com\/zh\/wp-json\/wp\/v2\/categories?post=18529"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/www.meetyoucarbide.com\/zh\/wp-json\/wp\/v2\/tags?post=18529"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}